Synthesis in millireactor system and stability of intermediates for the functionalization of imidazole

Perugini, Francesco (2015) Synthesis in millireactor system and stability of intermediates for the functionalization of imidazole. [Laurea magistrale], Università di Bologna, Corso di Studio in Chimica industriale [LM-DM270], Documento ad accesso riservato.
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Abstract

This Master thesis presents the results obtained in the curricular traineeship, carried out within the laboratories of the Department of Chemistry of the University of Bergen, during the Erasmus period, and within the Department of Industrial Chemistry of the University of Bologna. The project followed in Bergen concerned the synthesis of key intermediates used for the functionalization of the backbone of imidazole, using N,N'- diiodo-5,5-dimethylhydantoin (“DIH”) as an iodinating agent, and employing an innovative kind of chemical reactor: the “Multijet Oscillating Disc Millireactor” (MJOD Reactor). Afterwards, the work performed in Bologna consisted in verifying the stability in solution of the above mentioned N,N'-diiodo-5,5-dimethylhydantoin utilising spectrophotometric techniques and High Performance Liquid Chromatography analyses (HPLC).

Abstract
Tipologia del documento
Tesi di laurea (Laurea magistrale)
Autore della tesi
Perugini, Francesco
Relatore della tesi
Scuola
Corso di studio
Parole chiave
flow reactor DIH spectrophotometry HPLC
Data di discussione della Tesi
27 Marzo 2015
URI

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